<actionList title="preparation of silanols"> <p>This is a conversion of a chemical synthesis to STMML. We have deliberately not marked up the chemistry in this example!</p> <action title="step2"> <p>Take 1 mmol of the diol and dissolve in dioxan in <object title="flask"> <scalar title="volume" units="units:ml">25</scalar> </object> </p> </action> <action title="step2"> <p>Place flask in water bath with magnetic stirrer</p> </action> <!-- wait until certain condition --> <actionList endCondition="bath temperature stabilised"/> <action title="step3"> <p>Add 0.5 ml 1 M H2SO4</p> </action> <!-- carry out reaction --> <actionList endCondition="reaction complete; no diol spot remains on TLC"> <actionList title="check tlc"> <!-- wait for half an hour --> <action duration="half an hour"/> <action title="tlc"> <p>extract solution and check diol spot on TLC</p> </action> </actionList> </actionList> <!-- work up reaction --> <action title="step5"> <p>Add 10 ml water to flask</p> </action> <action title="step6"> <p>Neutralize acid with 10% NaHCO3</p> </action> <action title="step7" count="3"> <p>Extract with 10ml ether</p> </action> <action title="step8"> <p>Combine ether layers</p> </action> <action title="step9" count="2"> <p>Wash ether with 10 ml water</p> </action> <action title="step10"> <p>Wash ether with 10 ml saturated NaCl</p> </action> <action title="step11"> <p>Dry over anhydrous Na2SO4 and remove solvent on rotary evaporator</p> </action> </actionList>